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Beilstein J. Org. Chem. 2013, 9, 827–831, doi:10.3762/bjoc.9.94
Graphical Abstract
Scheme 1: Synthesis of fluorescent cyclodextrin 3 by click-chemistry.
Figure 1: 1H NMR-ROESY spectrum of the modified CD 3.
Figure 2: UV–vis spectrum of 3 (4 × 10−4 M) with and without a 10-fold excess of potassium adamantane-1-carbo...
Figure 3: Fluorescence spectrum of 3 (4 × 10−4 M) with and without a 10-fold excess of 1-adamantanecarboxylic...
Figure 4: DLS measurement of 3 with and without a 10-fold excess of potassium adamantane-1-carboxylate; black...
Figure 5: AF4 elution diagram of 3.
Beilstein J. Org. Chem. 2012, 8, 1929–1935, doi:10.3762/bjoc.8.224
Scheme 1: CTP of 1 and end-group functionalization with 5 yielding the azo-dye-end-group-labeled polymer 6.
Figure 1: Absorption spectra of 6 in water in a pH range from 7 to 2 (A). Absorption spectra of 6 in water de...
Figure 2: LCST measurements of 6, the complex of 6 and RAMEB-CD, and in comparison to pure PNIPAM.
Figure 3: Hydrodynamic diameters of 6, 7 and 8 (1 mg/mL) at 20 °C.
Figure 4: z-Average diameter (DZ) of the complex 8 in water as a function of temperature (0.5 mg/mL, heating ...